TBT/T3192-2008壓漿劑壓力泌水試驗儀現貨

TBT/T3192-2008壓漿劑壓力泌水試驗儀現貨砂漿壓(ya)(ya)力(li)泌(mi)水率試驗(yan)儀(yi)符合TBT/T3192-2008中華人民(min)共和(he)國鐵道行業標準(zhun)《鐵路后張法預應(ying)力(li)混(hun)凝土(tu)梁管道壓(ya)(ya)漿技術條件》。儀(yi)器內部直徑(jing)：50mm，試筒高度：200mm，儲水室(shi)：20mm，泌(mi)水口(kou)直徑(jing)：10mm，濾網直徑(jing)：0.08mm。，帶壓(ya)(ya)力(li)表。

1 一個包含２塊壓力表的CO2氣瓶，外測壓力表小分度值不應大于0.02 MPa，級別為1.5級。

2 壓力泌水容器為圓柱型不銹鋼壓力容器，需要進行壓力實驗，在0.8 MPa壓力下不會破裂。其尺寸如圖D.1所示。

 適(shi)(shi)用(yong)(yong)范圍主(zhu)(zhu)(zhu)(zhu)要適(shi)(shi)用(yong)(yong)于(yu)(yu)離(li)心(xin)分(fen)(fen)(fen)離(li)法(fa)(fa)(fa)測定(ding)粘(zhan)稠石(shi)(shi)油瀝(li)(li)(li)(li)(li)(li)青(qing)(qing)(qing)(qing)拌制(zhi)的(de)(de)(de)(de)(de)(de)(de)(de)(de)(de)瀝(li)(li)(li)(li)(li)(li)青(qing)(qing)(qing)(qing)混(hun)合(he)(he)(he)(he)料(liao)(liao)(liao)(liao)(liao)(liao)(liao)(liao)(liao)(liao)中(zhong)(zhong)(zhong)瀝(li)(li)(li)(li)(li)(li)青(qing)(qing)(qing)(qing)含(han)(han)量(liang)(liang)(liang)(liang)(liang)（或(huo)(huo)油石(shi)(shi)比），以(yi)評定(ding)路(lu)(lu)(lu)面(mian)(mian)施工(gong)(gong)時(shi)(shi)(shi)商品瀝(li)(li)(li)(li)(li)(li)青(qing)(qing)(qing)(qing)的(de)(de)(de)(de)(de)(de)(de)(de)(de)(de)質(zhi)(zhi)量(liang)(liang)(liang)(liang)(liang)，也(ye)適(shi)(shi)用(yong)(yong)于(yu)(yu)舊(jiu)路(lu)(lu)(lu)調查時(shi)(shi)(shi)檢(jian)測瀝(li)(li)(li)(li)(li)(li)青(qing)(qing)(qing)(qing)及(ji)瀝(li)(li)(li)(li)(li)(li)青(qing)(qing)(qing)(qing)混(hun)合(he)(he)(he)(he)料(liao)(liao)(liao)(liao)(liao)(liao)(liao)(liao)(liao)(liao)的(de)(de)(de)(de)(de)(de)(de)(de)(de)(de)瀝(li)(li)(li)(li)(li)(li)青(qing)(qing)(qing)(qing)用(yong)(yong)量(liang)(liang)(liang)(liang)(liang)。儀(yi)器(qi)(qi)(qi)(qi)符合(he)(he)(he)(he)交(jiao)(jiao)(jiao)通(tong)(tong)行(xing)業（公(gong)路(lu)(lu)(lu)瀝(li)(li)(li)(li)(li)(li)青(qing)(qing)(qing)(qing)混(hun)合(he)(he)(he)(he)料(liao)(liao)(liao)(liao)(liao)(liao)(liao)(liao)(liao)(liao)及(ji)瀝(li)(li)(li)(li)(li)(li)青(qing)(qing)(qing)(qing)混(hun)合(he)(he)(he)(he)料(liao)(liao)(liao)(liao)(liao)(liao)(liao)(liao)(liao)(liao)試(shi)(shi)(shi)(shi)驗規(gui)程）（JTJ052-93）中(zhong)(zhong)(zhong)瀝(li)(li)(li)(li)(li)(li)青(qing)(qing)(qing)(qing)混(hun)合(he)(he)(he)(he)料(liao)(liao)(liao)(liao)(liao)(liao)(liao)(liao)(liao)(liao)中(zhong)(zhong)(zhong)瀝(li)(li)(li)(li)(li)(li)青(qing)(qing)(qing)(qing)含(han)(han)量(liang)(liang)(liang)(liang)(liang)試(shi)(shi)(shi)(shi)驗（離(li)心(xin)分(fen)(fen)(fen)離(li)法(fa)(fa)(fa)）（T0722-93）所規(gui)定(ding)之技術指標，是公(gong)路(lu)(lu)(lu)交(jiao)(jiao)(jiao)通(tong)(tong)行(xing)業施工(gong)(gong)單位、試(shi)(shi)(shi)(shi)驗室(shi)、科研單位及(ji)教學(xue)機(ji)(ji)(ji)構的(de)(de)(de)(de)(de)(de)(de)(de)(de)(de)的(de)(de)(de)(de)(de)(de)(de)(de)(de)(de)*設(she)備二、主(zhu)(zhu)(zhu)(zhu)要技術參(can)數盛(sheng)料(liao)(liao)(liao)(liao)(liao)(liao)(liao)(liao)(liao)(liao)桶(tong)(tong)(tong)(tong)(tong)(tong)(tong)容量(liang)(liang)(liang)(liang)(liang)：1.5L盛(sheng)料(liao)(liao)(liao)(liao)(liao)(liao)(liao)(liao)(liao)(liao)桶(tong)(tong)(tong)(tong)(tong)(tong)(tong)轉(zhuan)(zhuan)速（可調）：3000r/min整機(ji)(ji)(ji)功(gong)率(lv)：400W電(dian)源：50HZ AC220V凈重(zhong)(zhong)(zhong)：30kg主(zhu)(zhu)(zhu)(zhu)機(ji)(ji)(ji)外(wai)(wai)形尺寸（直(zhi)徑(jing)××高）：390×510,,三、結(jie)構原(yuan)理儀(yi)器(qi)(qi)(qi)(qi)由機(ji)(ji)(ji)座(zuo)、電(dian)機(ji)(ji)(ji)、主(zhu)(zhu)(zhu)(zhu)軸(zhou)、盛(sheng)料(liao)(liao)(liao)(liao)(liao)(liao)(liao)(liao)(liao)(liao)桶(tong)(tong)(tong)(tong)(tong)(tong)(tong)、圓(yuan)(yuan)環(huan)形濾(lv)(lv)紙、手(shou)動(dong)裝(zhuang)(zhuang)(zhuang)置(zhi)(zhi)，外(wai)(wai)罩(zhao)(zhao)(zhao)和(he)電(dian)氣控制(zhi)器(qi)(qi)(qi)(qi)等組成(cheng)。 機(ji)(ji)(ji)座(zuo)為儀(yi)器(qi)(qi)(qi)(qi)的(de)(de)(de)(de)(de)(de)(de)(de)(de)(de)支(zhi)承(cheng)部分(fen)(fen)(fen)，電(dian)機(ji)(ji)(ji)、外(wai)(wai)罩(zhao)(zhao)(zhao)均安(an)(an)(an)裝(zhuang)(zhuang)(zhuang)其上(shang)(shang)(shang)(shang)。機(ji)(ji)(ji)座(zuo)的(de)(de)(de)(de)(de)(de)(de)(de)(de)(de)下(xia)(xia)(xia)沿(yan)有中(zhong)(zhong)(zhong)心(xin)距為300mm,4 個均布的(de)(de)(de)(de)(de)(de)(de)(de)(de)(de)9mm孔，用(yong)(yong)以(yi)儀(yi)器(qi)(qi)(qi)(qi)固定(ding)就(jiu)位。 盛(sheng)料(liao)(liao)(liao)(liao)(liao)(liao)(liao)(liao)(liao)(liao)桶(tong)(tong)(tong)(tong)(tong)(tong)(tong)安(an)(an)(an)裝(zhuang)(zhuang)(zhuang)在(zai)(zai)儀(yi)器(qi)(qi)(qi)(qi)的(de)(de)(de)(de)(de)(de)(de)(de)(de)(de)主(zhu)(zhu)(zhu)(zhu)軸(zhou)上(shang)(shang)(shang)(shang)，通(tong)(tong)過主(zhu)(zhu)(zhu)(zhu)軸(zhou)上(shang)(shang)(shang)(shang)的(de)(de)(de)(de)(de)(de)(de)(de)(de)(de)撥銷(xiao)帶動(dong)其旋(xuan)轉(zhuan)(zhuan)。電(dian)機(ji)(ji)(ji)出(chu)軸(zhou)與(yu)(yu)主(zhu)(zhu)(zhu)(zhu)軸(zhou)相(xiang)連，盛(sheng)料(liao)(liao)(liao)(liao)(liao)(liao)(liao)(liao)(liao)(liao)桶(tong)(tong)(tong)(tong)(tong)(tong)(tong)工(gong)(gong)作(zuo)上(shang)(shang)(shang)(shang)緣與(yu)(yu)上(shang)(shang)(shang)(shang)蓋間安(an)(an)(an)放(fang)(fang)圓(yuan)(yuan)環(huan)形濾(lv)(lv)紙，工(gong)(gong)作(zuo)前須(xu)(xu)用(yong)(yong)并帽擰緊(jin)，使(shi)(shi)(shi)桶(tong)(tong)(tong)(tong)(tong)(tong)(tong)與(yu)(yu)上(shang)(shang)(shang)(shang)蓋緊(jin)固。主(zhu)(zhu)(zhu)(zhu)軸(zhou)上(shang)(shang)(shang)(shang)端生入(ru)(ru)外(wai)(wai)罩(zhao)(zhao)(zhao)上(shang)(shang)(shang)(shang)罩(zhao)(zhao)(zhao)的(de)(de)(de)(de)(de)(de)(de)(de)(de)(de)軸(zhou)承(cheng)支(zhi)承(cheng)中(zhong)(zhong)(zhong)，保(bao)證(zheng)(zheng)盛(sheng)料(liao)(liao)(liao)(liao)(liao)(liao)(liao)(liao)(liao)(liao)桶(tong)(tong)(tong)(tong)(tong)(tong)(tong)工(gong)(gong)作(zuo)時(shi)(shi)(shi)旋(xuan)轉(zhuan)(zhuan)平(ping)穩(wen)。，飛(fei)濺。下(xia)(xia)(xia)罩(zhao)(zhao)(zhao)上(shang)(shang)(shang)(shang)設(she)有檠動(dong)裝(zhuang)(zhuang)(zhuang)置(zhi)(zhi)，扳(ban)動(dong)手(shou)柄(bing) ，可使(shi)(shi)(shi)斷電(dian)后(hou)的(de)(de)(de)(de)(de)(de)(de)(de)(de)(de)電(dian)機(ji)(ji)(ji)盛(sheng)料(liao)(liao)(liao)(liao)(liao)(liao)(liao)(liao)(liao)(liao)桶(tong)(tong)(tong)(tong)(tong)(tong)(tong)在(zai)(zai)較短(duan)的(de)(de)(de)(de)(de)(de)(de)(de)(de)(de)時(shi)(shi)(shi)間內停(ting)轉(zhuan)(zhuan)，下(xia)(xia)(xia)罩(zhao)(zhao)(zhao)一(yi)側設(she)有排(pai)(pai)液(ye)(ye)口以(yi)排(pai)(pai)出(chu)溶(rong)(rong)(rong)(rong)液(ye)(ye)。上(shang)(shang)(shang)(shang)罩(zhao)(zhao)(zhao)與(yu)(yu)下(xia)(xia)(xia)罩(zhao)(zhao)(zhao)見緊(jin)密配合(he)(he)(he)(he)。并安(an)(an)(an)裝(zhuang)(zhuang)(zhuang)兩調節搭扣和(he)耐酸(suan)堿橡膠密封圈以(yi)保(bao)證(zheng)(zheng)試(shi)(shi)(shi)(shi)驗時(shi)(shi)(shi)溶(rong)(rong)(rong)(rong)液(ye)(ye)全部回收(shou)。上(shang)(shang)(shang)(shang)罩(zhao)(zhao)(zhao)上(shang)(shang)(shang)(shang)方有加(jia)(jia)(jia)液(ye)(ye)孔，供加(jia)(jia)(jia)新溶(rong)(rong)(rong)(rong)液(ye)(ye)用(yong)(yong)。電(dian)器(qi)(qi)(qi)(qi)控制(zhi)器(qi)(qi)(qi)(qi)與(yu)(yu)主(zhu)(zhu)(zhu)(zhu)機(ji)(ji)(ji)通(tong)(tong)過插座(zuo)相(xiang)連。電(dian)機(ji)(ji)(ji)調速為可控硅(gui)電(dian)壓無級調速。四、儀(yi)器(qi)(qi)(qi)(qi)的(de)(de)(de)(de)(de)(de)(de)(de)(de)(de)安(an)(an)(an)裝(zhuang)(zhuang)(zhuang)儀(yi)器(qi)(qi)(qi)(qi)必須(xu)(xu)安(an)(an)(an)裝(zhuang)(zhuang)(zhuang)在(zai)(zai)堅固的(de)(de)(de)(de)(de)(de)(de)(de)(de)(de)混(hun)凝土地面(mian)(mian)（或(huo)(huo)基礎(chu)）上(shang)(shang)(shang)(shang)，并保(bao)證(zheng)(zheng)主(zhu)(zhu)(zhu)(zhu)軸(zhou)鉛(qian)垂放(fang)(fang)置(zhi)(zhi)，必要時(shi)(shi)(shi)可利用(yong)(yong)機(ji)(ji)(ji)座(zuo)安(an)(an)(an)裝(zhuang)(zhuang)(zhuang)孔4 -M8膨脹螺栓將(jiang)主(zhu)(zhu)(zhu)(zhu)機(ji)(ji)(ji)固定(ding)。 儀(yi)器(qi)(qi)(qi)(qi)使(shi)(shi)(shi)用(yong)(yong)50HZ 220V交(jiao)(jiao)(jiao)流電(dian)，使(shi)(shi)(shi)用(yong)(yong)單相(xiang)三腳扁插座(zuo)，接(jie)(jie)地應可靠(kao)。五、試(shi)(shi)(shi)(shi)驗步驟(zou)（操(cao)作(zuo)方法(fa)(fa)(fa)）1、向(xiang)裝(zhuang)(zhuang)(zhuang)有試(shi)(shi)(shi)(shi)樣(yang)的(de)(de)(de)(de)(de)(de)(de)(de)(de)(de)燒(shao)(shao)(shao)杯中(zhong)(zhong)(zhong)（也(ye)可直(zhi)接(jie)(jie)在(zai)(zai)盛(sheng)料(liao)(liao)(liao)(liao)(liao)(liao)(liao)(liao)(liao)(liao)桶(tong)(tong)(tong)(tong)(tong)(tong)(tong)中(zhong)(zhong)(zhong)）注入(ru)(ru)三氯乙稀溶(rong)(rong)(rong)(rong)液(ye)(ye)（工(gong)(gong)業用(yong)(yong)），將(jiang)試(shi)(shi)(shi)(shi)件浸沒，記(ji)錄溶(rong)(rong)(rong)(rong)劑(ji)用(yong)(yong)量(liang)(liang)(liang)(liang)(liang)。浸泡30分(fen)(fen)(fen)鐘后(hou)，用(yong)(yong)玻璃棒適(shi)(shi)當攪動(dong)混(hun)合(he)(he)(he)(he)料(liao)(liao)(liao)(liao)(liao)(liao)(liao)(liao)(liao)(liao)，使(shi)(shi)(shi)瀝(li)(li)(li)(li)(li)(li)青(qing)(qing)(qing)(qing)充分(fen)(fen)(fen)溶(rong)(rong)(rong)(rong)解。2、將(jiang)混(hun)合(he)(he)(he)(he)料(liao)(liao)(liao)(liao)(liao)(liao)(liao)(liao)(liao)(liao)及(ji)溶(rong)(rong)(rong)(rong)液(ye)(ye)倒如(ru)盛(sheng)料(liao)(liao)(liao)(liao)(liao)(liao)(liao)(liao)(liao)(liao)桶(tong)(tong)(tong)(tong)(tong)(tong)(tong)中(zhong)(zhong)(zhong)，用(yong)(yong)少量(liang)(liang)(liang)(liang)(liang)溶(rong)(rong)(rong)(rong)劑(ji)將(jiang)燒(shao)(shao)(shao)杯及(ji)玻璃棒上(shang)(shang)(shang)(shang)的(de)(de)(de)(de)(de)(de)(de)(de)(de)(de)粘(zhan)附(fu)物(wu)全部裝(zhuang)(zhuang)(zhuang)入(ru)(ru)盛(sheng)料(liao)(liao)(liao)(liao)(liao)(liao)(liao)(liao)(liao)(liao)桶(tong)(tong)(tong)(tong)(tong)(tong)(tong)中(zhong)(zhong)(zhong)。3、稱(cheng)(cheng)(cheng)取(qu)(qu)(qu)(qu)(qu)潔凈的(de)(de)(de)(de)(de)(de)(de)(de)(de)(de)圓(yuan)(yuan)環(huan)形濾(lv)(lv)紙質(zhi)(zhi)量(liang)(liang)(liang)(liang)(liang)，精確(que)(que)至(zhi)(zhi)0.01g（注意：濾(lv)(lv)紙不宜反復多次使(shi)(shi)(shi)用(yong)(yong)，有石(shi)(shi)粉(fen)粘(zhan)附(fu)時(shi)(shi)(shi)應用(yong)(yong)毛刷刷盡）。4、將(jiang)濾(lv)(lv)紙墊在(zai)(zai)盛(sheng)料(liao)(liao)(liao)(liao)(liao)(liao)(liao)(liao)(liao)(liao)桶(tong)(tong)(tong)(tong)(tong)(tong)(tong)上(shang)(shang)(shang)(shang)緣。加(jia)(jia)(jia)蓋緊(jin)固。在(zai)(zai)外(wai)(wai)罩(zhao)(zhao)(zhao)排(pai)(pai)液(ye)(ye)口下(xia)(xia)(xia)放(fang)(fang)置(zhi)(zhi)容量(liang)(liang)(liang)(liang)(liang)大于(yu)(yu)1700ml的(de)(de)(de)(de)(de)(de)(de)(de)(de)(de)回收(shou)瓶(ping)，并蓋上(shang)(shang)(shang)(shang)外(wai)(wai)罩(zhao)(zhao)(zhao)上(shang)(shang)(shang)(shang)罩(zhao)(zhao)(zhao)的(de)(de)(de)(de)(de)(de)(de)(de)(de)(de)加(jia)(jia)(jia)液(ye)(ye)孔。5、接(jie)(jie)通(tong)(tong)電(dian)源，啟動(dong)惦記(ji)，旋(xuan)轉(zhuan)(zhuan)旋(xuan)鈕，使(shi)(shi)(shi)電(dian)機(ji)(ji)(ji)及(ji)盛(sheng)料(liao)(liao)(liao)(liao)(liao)(liao)(liao)(liao)(liao)(liao)桶(tong)(tong)(tong)(tong)(tong)(tong)(tong)轉(zhuan)(zhuan)素逐步增值(zhi)(zhi)300r/min以(yi)上(shang)(shang)(shang)(shang)。此(ci)時(shi)(shi)(shi)瀝(li)(li)(li)(li)(li)(li)青(qing)(qing)(qing)(qing)溶(rong)(rong)(rong)(rong)液(ye)(ye)將(jiang)通(tong)(tong)過排(pai)(pai)液(ye)(ye)口注入(ru)(ru)回收(shou)瓶(ping)中(zhong)(zhong)(zhong)，待流完后(hou)停(ting)機(ji)(ji)(ji)。6、從上(shang)(shang)(shang)(shang)罩(zhao)(zhao)(zhao)上(shang)(shang)(shang)(shang)方加(jia)(jia)(jia)液(ye)(ye)孔中(zhong)(zhong)(zhong)加(jia)(jia)(jia)入(ru)(ru)新溶(rong)(rong)(rong)(rong)液(ye)(ye)，用(yong)(yong)量(liang)(liang)(liang)(liang)(liang)相(xiang)等。稍停(ting)5分(fen)(fen)(fen)鐘后(hou)，重(zhong)(zhong)(zhong)復以(yi)上(shang)(shang)(shang)(shang)5”操(cao)作(zuo)。如(ru)此(ci)數次直(zhi)到流出(chu)的(de)(de)(de)(de)(de)(de)(de)(de)(de)(de)溶(rong)(rong)(rong)(rong)液(ye)(ye)成(cheng)清澈的(de)(de)(de)(de)(de)(de)(de)(de)(de)(de)淡黃(huang)色為止。7、停(ting)機(ji)(ji)(ji)。取(qu)(qu)(qu)(qu)(qu)下(xia)(xia)(xia)上(shang)(shang)(shang)(shang)罩(zhao)(zhao)(zhao)及(ji)盛(sheng)料(liao)(liao)(liao)(liao)(liao)(liao)(liao)(liao)(liao)(liao)桶(tong)(tong)(tong)(tong)(tong)(tong)(tong)上(shang)(shang)(shang)(shang)蓋，再(zai)仔細取(qu)(qu)(qu)(qu)(qu)下(xia)(xia)(xia)圓(yuan)(yuan)環(huan)形濾(lv)(lv)紙，在(zai)(zai)通(tong)(tong)風櫥或(huo)(huo)室(shi)內蒸發干(gan)(gan)燥(zao)(zao)，然后(hou)放(fang)(fang)入(ru)(ru)105±5的(de)(de)(de)(de)(de)(de)(de)(de)(de)(de)烘(hong)箱中(zhong)(zhong)(zhong)干(gan)(gan)燥(zao)(zao)，稱(cheng)(cheng)(cheng)取(qu)(qu)(qu)(qu)(qu)質(zhi)(zhi)量(liang)(liang)(liang)(liang)(liang)，其增重(zhong)(zhong)(zhong)部分(fen)(fen)(fen)（m）為礦粉(fen)的(de)(de)(de)(de)(de)(de)(de)(de)(de)(de)一(yi)部分(fen)(fen)(fen)。8、將(jiang)盛(sheng)料(liao)(liao)(liao)(liao)(liao)(liao)(liao)(liao)(liao)(liao)桶(tong)(tong)(tong)(tong)(tong)(tong)(tong)中(zhong)(zhong)(zhong)集料(liao)(liao)(liao)(liao)(liao)(liao)(liao)(liao)(liao)(liao)仔細取(qu)(qu)(qu)(qu)(qu)出(chu)，在(zai)(zai)通(tong)(tong)風櫥或(huo)(huo)室(shi)內蒸發后(hou)放(fang)(fang)入(ru)(ru)105±5的(de)(de)(de)(de)(de)(de)(de)(de)(de)(de)烘(hong)箱中(zhong)(zhong)(zhong)烘(hong)干(gan)(gan)（一(yi)般需要4小(xiao)時(shi)(shi)(shi)），然后(hou)放(fang)(fang)入(ru)(ru)大干(gan)(gan)燥(zao)(zao)器(qi)(qi)(qi)(qi)中(zhong)(zhong)(zhong)冷至(zhi)(zhi)室(shi)溫，稱(cheng)(cheng)(cheng)取(qu)(qu)(qu)(qu)(qu)集料(liao)(liao)(liao)(liao)(liao)(liao)(liao)(liao)(liao)(liao)質(zhi)(zhi)量(liang)(liang)(liang)(liang)(liang)（m1）9、用(yong)(yong)壓力過濾(lv)(lv)器(qi)(qi)(qi)(qi)回收(shou)瓶(ping)中(zhong)(zhong)(zhong)的(de)(de)(de)(de)(de)(de)(de)(de)(de)(de)瀝(li)(li)(li)(li)(li)(li)青(qing)(qing)(qing)(qing)溶(rong)(rong)(rong)(rong)液(ye)(ye)，由濾(lv)(lv)液(ye)(ye)的(de)(de)(de)(de)(de)(de)(de)(de)(de)(de)增重(zhong)(zhong)(zhong)m取(qu)(qu)(qu)(qu)(qu)出(chu)泄(xie)漏入(ru)(ru)濾(lv)(lv)液(ye)(ye)中(zhong)(zhong)(zhong)的(de)(de)(de)(de)(de)(de)(de)(de)(de)(de)礦粉(fen)。如(ru)無壓力過濾(lv)(lv)器(qi)(qi)(qi)(qi)時(shi)(shi)(shi)，也(ye)可用(yong)(yong)燃(ran)(ran)燒(shao)(shao)(shao)法(fa)(fa)(fa)測定(ding)抽(chou)(chou)提(ti)(ti)液(ye)(ye)中(zhong)(zhong)(zhong)礦粉(fen)的(de)(de)(de)(de)(de)(de)(de)(de)(de)(de)質(zhi)(zhi)量(liang)(liang)(liang)(liang)(liang)的(de)(de)(de)(de)(de)(de)(de)(de)(de)(de)步驟(zou)如(ru)下(xia)(xia)(xia)：1、將(jiang)回收(shou)瓶(ping)中(zhong)(zhong)(zhong)的(de)(de)(de)(de)(de)(de)(de)(de)(de)(de)抽(chou)(chou)提(ti)(ti)液(ye)(ye)倒入(ru)(ru)量(liang)(liang)(liang)(liang)(liang)筒中(zhong)(zhong)(zhong)，準確(que)(que)定(ding)量(liang)(liang)(liang)(liang)(liang)至(zhi)(zhi)ml（v）2、充分(fen)(fen)(fen)攪勻抽(chou)(chou)提(ti)(ti)液(ye)(ye)，取(qu)(qu)(qu)(qu)(qu)出(chu)10ml（V）放(fang)(fang)入(ru)(ru)坩(gan)堝中(zhong)(zhong)(zhong)，在(zai)(zai)熱(re)浴上(shang)(shang)(shang)(shang)適(shi)(shi)當加(jia)(jia)(jia)熱(re)使(shi)(shi)(shi)溶(rong)(rong)(rong)(rong)液(ye)(ye) 試(shi)(shi)(shi)(shi)樣(yang)發成(cheng)暗黑色后(hou)，置(zhi)(zhi)高溫（500-600中(zhong)(zhong)(zhong)燒(shao)(shao)(shao)成(cheng)殘(can)渣(zha)，取(qu)(qu)(qu)(qu)(qu)出(chu)坩(gan)堝冷卻(que)3、向(xiang)坩(gan)堝中(zhong)(zhong)(zhong)按(an)每1g殘(can)渣(zha)5ml的(de)(de)(de)(de)(de)(de)(de)(de)(de)(de)用(yong)(yong)量(liang)(liang)(liang)(liang)(liang)比例，注入(ru)(ru)碳酸(suan)胺飽(bao)和(he)溶(rong)(rong)(rong)(rong)液(ye)(ye)，精置(zhi)(zhi)1小(xiao)時(shi)(shi)(shi)，放(fang)(fang)入(ru)(ru)入(ru)(ru)105±5烘(hong)箱中(zhong)(zhong)(zhong)干(gan)(gan)燥(zao)(zao)。4、取(qu)(qu)(qu)(qu)(qu)出(chu)放(fang)(fang)在(zai)(zai)干(gan)(gan)燥(zao)(zao)器(qi)(qi)(qi)(qi)中(zhong)(zhong)(zhong)冷卻(que)，稱(cheng)(cheng)(cheng)取(qu)(qu)(qu)(qu)(qu)殘(can)渣(zha)質(zhi)(zhi)量(liang)(liang)(liang)(liang)(liang)（m4）10、計算(suan)瀝(li)(li)(li)(li)(li)(li)青(qing)(qing)(qing)(qing)混(hun)合(he)(he)(he)(he)料(liao)(liao)(liao)(liao)(liao)(liao)(liao)(liao)(liao)(liao)中(zhong)(zhong)(zhong)礦粉(fen)的(de)(de)(de)(de)(de)(de)(de)(de)(de)(de)總質(zhi)(zhi)量(liang)(liang)(liang)(liang)(liang)為 m4=m1+m2+m3式(shi)中(zhong)(zhong)(zhong)：m4-瀝(li)(li)(li)(li)(li)(li)青(qing)(qing)(qing)(qing)混(hun)合(he)(he)(he)(he)料(liao)(liao)(liao)(liao)(liao)(liao)(liao)(liao)(liao)(liao)中(zhong)(zhong)(zhong)礦料(liao)(liao)(liao)(liao)(liao)(liao)(liao)(liao)(liao)(liao)部分(fen)(fen)(fen)的(de)(de)(de)(de)(de)(de)(de)(de)(de)(de)總質(zhi)(zhi)量(liang)(liang)(liang)(liang)(liang)（g）m1-盛(sheng)料(liao)(liao)(liao)(liao)(liao)(liao)(liao)(liao)(liao)(liao)桶(tong)(tong)(tong)(tong)(tong)(tong)(tong)中(zhong)(zhong)(zhong)留下(xia)(xia)(xia)的(de)(de)(de)(de)(de)(de)(de)(de)(de)(de)集料(liao)(liao)(liao)(liao)(liao)(liao)(liao)(liao)(liao)(liao)干(gan)(gan)燥(zao)(zao)質(zhi)(zhi)量(liang)(liang)(liang)(liang)(liang)（g）m2-圓(yuan)(yuan)環(huan)形濾(lv)(lv)紙試(shi)(shi)(shi)(shi)驗前后(hou)的(de)(de)(de)(de)(de)(de)(de)(de)(de)(de)增重(zhong)(zhong)(zhong)（g）m3-泄(xie)漏入(ru)(ru)抽(chou)(chou)提(ti)(ti)液(ye)(ye)中(zhong)(zhong)(zhong)的(de)(de)(de)(de)(de)(de)(de)(de)(de)(de)礦粉(fen)質(zhi)(zhi)量(liang)(liang)(liang)(liang)(liang)（g）用(yong)(yong)燃(ran)(ran)燒(shao)(shao)(shao)法(fa)(fa)(fa)時(shi)(shi)(shi)可按(an)下(xia)(xia)(xia)式(shi)計算(suan)式(shi)中(zhong)(zhong)(zhong)：Va-抽(chou)(chou)提(ti)(ti)液(ye)(ye)的(de)(de)(de)(de)(de)(de)(de)(de)(de)(de)總量(liang)(liang)(liang)(liang)(liang)（ml）Vb-取(qu)(qu)(qu)(qu)(qu)出(chu)的(de)(de)(de)(de)(de)(de)(de)(de)(de)(de)燃(ran)(ran)燒(shao)(shao)(shao)干(gan)(gan)燥(zao)(zao)的(de)(de)(de)(de)(de)(de)(de)(de)(de)(de)抽(chou)(chou)提(ti)(ti)液(ye)(ye)數量(liang)(liang)(liang)(liang)(liang)（ml m1-坩(gan)堝中(zhong)(zhong)(zhong)燃(ran)(ran)燒(shao)(shao)(shao)干(gan)(gan)燥(zao)(zao)的(de)(de)(de)(de)(de)(de)(de)(de)(de)(de)殘(can)渣(zha)質(zhi)(zhi)量(liang)(liang)(liang)(liang)(liang)（g）瀝(li)(li)(li)(li)(li)(li)青(qing)(qing)(qing)(qing)混(hun)合(he)(he)(he)(he)料(liao)(liao)(liao)(liao)(liao)(liao)(liao)(liao)(liao)(liao)中(zhong)(zhong)(zhong)瀝(li)(li)(li)(li)(li)(li)青(qing)(qing)(qing)(qing)含(han)(han)量(liang)(liang)(liang)(liang)(liang)按(an)下(xia)(xia)(xia)式(shi)計算(suan)式(shi)中(zhong)(zhong)(zhong)：m-瀝(li)(li)(li)(li)(li)(li)青(qing)(qing)(qing)(qing)混(hun)合(he)(he)(he)(he)料(liao)(liao)(liao)(liao)(liao)(liao)(liao)(liao)(liao)(liao)的(de)(de)(de)(de)(de)(de)(de)(de)(de)(de)總質(zhi)(zhi)量(liang)(liang)(liang)(liang)(liang)（g）Pb-瀝(li)(li)(li)(li)(li)(li)青(qing)(qing)(qing)(qing)混(hun)合(he)(he)(he)(he)料(liao)(liao)(liao)(liao)(liao)(liao)(liao)(liao)(liao)(liao)的(de)(de)(de)(de)(de)(de)(de)(de)(de)(de)瀝(li)(li)(li)(li)(li)(li)青(qing)(qing)(qing)(qing)含(han)(han)量(liang)(liang)(liang)(liang)(liang)（）Pa-瀝(li)(li)(li)(li)(li)(li)青(qing)(qing)(qing)(qing)混(hun)合(he)(he)(he)(he)料(liao)(liao)(liao)(liao)(liao)(liao)(liao)(liao)(liao)(liao)的(de)(de)(de)(de)(de)(de)(de)(de)(de)(de)油石(shi)(shi)比（）11、測試(shi)(shi)(shi)(shi)報(bao)告同(tong)一(yi)瀝(li)(li)(li)(li)(li)(li)青(qing)(qing)(qing)(qing)混(hun)合(he)(he)(he)(he)料(liao)(liao)(liao)(liao)(liao)(liao)(liao)(liao)(liao)(liao)式(shi)樣(yang)至(zhi)(zhi)少平(ping)行(xing)試(shi)(shi)(shi)(shi)驗兩次，取(qu)(qu)(qu)(qu)(qu)平(ping)均值(zhi)(zhi)作(zuo)為試(shi)(shi)(shi)(shi)驗結(jie)果，兩次試(shi)(shi)(shi)(shi)驗結(jie)果的(de)(de)(de)(de)(de)(de)(de)(de)(de)(de)差(cha)值(zhi)(zhi)應小(xiao)于(yu)(yu)0.3%，當大于(yu)(yu)0.3%但小(xiao)于(yu)(yu)0.5%時(shi)(shi)(shi)，應補充平(ping)行(xing)試(shi)(shi)(shi)(shi)驗一(yi)次，以(yi)3次試(shi)(shi)(shi)(shi)驗的(de)(de)(de)(de)(de)(de)(de)(de)(de)(de)平(ping)均值(zhi)(zhi)作(zuo)為試(shi)(shi)(shi)(shi)驗結(jie)構，3次試(shi)(shi)(shi)(shi)驗的(de)(de)(de)(de)(de)(de)(de)(de)(de)(de)大值(zhi)(zhi)和(he)小(xiao)值(zhi)(zhi)之差(cha)不得大于(yu)(yu)0.5%六、注意事(shi)項1、安(an)(an)(an)放(fang)(fang)儀(yi)器(qi)(qi)(qi)(qi)的(de)(de)(de)(de)(de)(de)(de)(de)(de)(de)室(shi)內必須(xu)(xu)通(tong)(tong)風，建(jian)議采用(yong)(yong)排(pai)(pai)風裝(zhuang)(zhuang)(zhuang)置(zhi)(zhi)。2、試(shi)(shi)(shi)(shi)驗結(jie)束(shu)打開上(shang)(shang)(shang)(shang)罩(zhao)(zhao)(zhao)時(shi)(shi)(shi)，必須(xu)(xu)確(que)(que)保(bao)電(dian)機(ji)(ji)(ji)及(ji)盛(sheng)料(liao)(liao)(liao)(liao)(liao)(liao)(liao)(liao)(liao)(liao)桶(tong)(tong)(tong)(tong)(tong)(tong)(tong)*停(ting)轉(zhuan)(zhuan)后(hou)方可進行(xing)

3 10mL的量筒。

、 試驗程序

1 根據5.2.1的要求攪拌制備漿體。

2 將攪拌好的漿體在自加水開始的7 min內倒入容積為400 mL的圓形過濾漏斗中，倒入的漿體體積為200 mL。